Hayden Johnson1, Thomas Yates1, Chidambaram Ramanathan2, Melissa Puppa2, Marie van der Merwe2, and Aaryani Tipirneni-Sajja1
1Biomedical Engineering, University of Memphis, Memphis, TN, United States, 2College of Health Sciences, University of Memphis, Memphis, TN, United States
Synopsis
NMR-based metabolomics is a powerful technique
for elucidating the metabolic effects of diet through the identification and
quantification of molecules present in tissues. This study utilizes time-domain
processing of NMR data for robust, reproducible resonance characterization in
the profiling of lipid species in heart and liver tissues of male and female animals
subject to high fat diets with and without time-restriction. Results show triglyceride
and fatty acid accumulation was associated with eating a high fat diet, but these
effects were attenuated by time-restricted feeding. Hepatic lipids expressed a
sexually dimorphic response, with higher concentrations of many lipids in female
subjects.
Introduction
NMR-based metabolomics is conventionally performed in the frequency-domain which
requires many user-dependent steps such as zero-filling, apodization, phase
and baseline correction followed by quantification by integration or peak deconvolution and hence,
can introduce user bias and inter-operator variability in metabolite
quantification1. In
this study, we utilize a Bayesian approach to time-domain NMR parameter
estimation, CRAFT (Complete Reduction to Amplitude-Frequency Table), for
accurate, time-efficient quantification of lipid metabolites in rat tissue
samples. These rats were subjects of a dietary study examining time-restricted
feeding (TRF), an increasingly popular diet in which caloric intake is restricted
to a certain window of time each day. Recent research suggests TRF can be an
effective strategy for weight loss and preventing common chronic metabolic
diseases such as obesity and type 2 diabetes; however, most studies to date only
examine male animals2,3. This study investigates both sexes, as
males and females handle many major metabolic challenges such as fat storage
and energy homeostasis differently4. Liver and heart tissues were profiled
to evaluate the effects of diet as these organs play major roles in maintaining
systemic metabolic homeostasis.Methods
Male and female Nile grass rats were subjects of a TRF study on one of
four diets (chow ad libitum, high fat ad libitum [HF-AD], high fat morning TRF [HF-AM],
and high fat evening TRF [HF-EV]). The TRF restrictions were characterized by access
to the high fat diet for the first 6 hours of the 12 hour light/active phase for
HF-AM or the second 6 hours of the 12 hour light/active phase for HF-PM. Hepatic
and cardiac tissues were harvested after six weeks, and lipids were extracted
from tissues using an MTBE extraction before resolubilizing in deuterated
solvent mixture (chloroform, methanol, and water) for profiling by proton NMR
using a 400-MHz JEOL ECZ NMR spectrometer. For all measurements, the
spectrometer was cooled to 0°C to shift the water resonance and 32 scans were
recorded using a single-pulse proton sequence with a pulse angle of 45° and a
relaxation delay of 4 s. NMR data processing for all samples was performed in
JEOL Delta v5.3 software using CRAFT. Resonances used for quantification of lipid
groups were first identified using reference standards and using relevant
scientific publications5,6. Lipid species quantified include total triglycerides, total
cholesterol, total fatty acids (TFA), unsaturated fatty acids (UFA), omega-3
fatty acids, linoleic acid, phosphatidylcholine (PC), phosphatidylethanolamine,
and sphingomyelin. Two-way ANOVA with Holm-Sidak post-hoc testing (Sigma Plot
14.5) was used to compare tissue-specific metabolite concentrations between sexes
and diets – with separate analysis performed to independently examine the
effects of the high fat diet (Chow vs. HF-AD) and TRF (HF-AD vs. HF-AM vs.
HF-EV). For both liver and heart lipid profiles, hierarchical clustering analysis
(HCA) with heatmaps for visualization was performed including all dietary
groups using MetaboAnalyst software (https://www.metaboanalyst.ca) using
auto-scaled data (mean-subtracted and divided by standard deviation).Results & Discussion
Representative hepatic and cardiac lipid spectra
are displayed in figure 1. As expected, rats on the HF-AD diet expressed a
significantly greater amount of many hepatic lipid species compared to those on
the standard chow diet including triglycerides, cholesterol, TFA, and UFA (Table
1). Similar increases were seen in cardiac tissue of HF-AD rats for
triglycerides, TFA, UFA, and PC. Both the HF-AM and HF-EV diet schedules were associated with lower levels of many of these
lipids associated with high fat diet (Table 2). In both heart and liver
tissues, significantly lower concentrations of TFA and UFA were measured in each
TRF group compared to their ad libitum counterpart. Although both tissues also
exhibited lower triglyceride levels in response to TRF, this effect was only
statistically significantly levels for hepatic triglycerides in the HF-AM
dietary group. Irrespective of diet, females expressed significantly higher
levels of many lipid groups including triglycerides, TFA, UFA, and omega-3
fatty acids in the liver, an effect which was not seen in heart samples. The higher
concentrations of hepatic lipids measured in females compared to males suggest
a sexual dimorphism in hepatic metabolism. Visualization of these trends is
aided by the heatmaps of figures 2 and 3 – such as the many red blocks
representing high levels of triglycerides and fatty acids in the HF-AD diets in
both figures, or the red-field at the bottom half of figure 2 representing the high
amounts of many lipid species in the livers of female rats compared to males.Conclusion
The metabolite profiles measured using the CRAFT approach for time-domain NMR parameter
estimation suggest that TRF induces positive effects on lipid metabolism. Acknowledgements
No acknowledgement found.References
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