Directional and anisotropy measures from a diffusion model composed of VERDICT compartments were compared with directional and anisotropy measures from structure tensor analysis of registered histology images. A significant positive correlation was found between the direction of the Zeppelin component of the diffusion model (assumed to represent the extracellular space) and the predominant direction of the structure tensor from the stroma, where the primary feature is aligned collagen. The correlation of anisotropy measures was weak, which may be due to difficulties in detecting alignment in regions with densely-packed collagen, which have nearly uniform intensity on H&E staining.
MR acquisition and fitting
Seven formalin-fixed tissue samples containing invasive breast cancers were rehydrated with saline and scanned at 9.4 T (Varian Inc). The protocol10 consisted of 42 diffusion-weighted images (0.25 x 0.25 x 0.5 mm3, 3 gradient directions + 1 unweighted), bmax=21 960 s/mm2 and gradient separations from 10-80 ms. Two DTIs (42 directions + 6 unweighted), b=1000 and 1500 s/mm2 were also acquired. A fast spin echo (fSE, 0.125 x 0.125 x 0.5 mm3) was acquired for registration. Data were fitted voxelwise to a Zeppelin-Sphere model (cylindrically symmetric tensor + restricted isotropic diffusion)9.
Histology and structure tensor analysis
Three micron slices were cut every 100 µm and stained with H&E. Slides were digitised (Hamamatsu Nanozoomer) at 20x magnification.
ST analysis was conducted at 5x magnification using the freely available Structure Tensor Toolbox8. The ST describes the local image-texture orientation by convolving the image with a 2D Gaussian weighting function over a neighbourhood7,8. The Gaussian full width at half maximum used was 15 µm, approximately the distance a water molecule is expected to diffuse over a 30 ms experiment. Analysis was restricted to the extracellular space by a mask of the stroma obtained via k-means clustering.
An anisotropy index was calculated using the eigenvalues λ1≥λ2 of the structure tensor: $$$AI=\frac{\lambda_1-\lambda_2}{\lambda_1+\lambda_2}$$$. The eigenvector of λ2 gives the dominant direction.
Image registration and correlation
Adjacent slices were stacked at 100 µm intervals into a 3D volume using 2D pairwise rigid registration with a block-matching strategy11,12 and correlation coefficient as similarity measure. The 3D stack was registered to the fSE volume using an intensity-based affine registration from ITK13 with normalized mutual information as similarity metric. The resulting transformation was applied to the diffusion parametric maps and directional vectors.
ST results were downsampled to the MRI resolution, normalizing AI by stromal area to reflect extracellular anisotropy. The Zeppelin component of the diffusion model was assumed to represent the extracellular space. The 3D MRI vectors were projected into the 2D histological plane (from registration) for comparison.
Direction of the Zeppelin projection (φ) and fractional anisotropy (FA) were compared to ST direction and AI, averaging over a 5x5 window around each pixel. Pearson correlation coefficients were calculated, weighting the direction regression by the FA from MRI to limit the influence of nearly isotropic pixels with uncertain directions.
Figure 1 shows the registration.
Figure 2 demonstrates the results of the structure tensor analysis.
Registered sections of the ST and diffusion directional analysis are shown in Figure 3 for one sample.
Figure 4 depicts the correlations between MRI and histology for both the direction and anisotropy measures. There is a significant positive correlation between the dominant directions directions of MRI and ST. The correlation plots demonstrate quite large variance. This is likely due to errors in the registration, which affect both the pixel locations for comparison and the pixel value φ, calculated when the transformation is applied to the diffusion vectors.
The anisotropy correlation is weaker. This may be due to difficulties capturing orientation of dense collagen (Figure 5). Tightly packed collagen demonstrates less intensity variation in the histology images, producing AI estimates that may be low even when collagen anisotropy is high (visible as the spread in AI as FA increases in the bottom left plot of Figure 4). Additionally, AI measures the gradient in the stroma, where the dominant feature is collagen orientation, while FA measures the hindrance of water, which may result from structures other than collagen.
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