Breathing hyperoxic gas results in dissolved oxygen in blood plasma, shortening T1 of arterial blood (T1a). Quantification of T1a is difficult due to blood flow between the inversion and acquisition. Here, this problem is overcome using an intermittent cuff occlusion protocol to suspend flow in the femoral artery and vein. An inversion recovery-prepared bSSFP sequence was used to measure T1a during normoxia (FiO2=21% O2) and graded hyperoxia (FiO2~33%, 48%, 55%, 100% O2) in ten healthy subjects at 3T. During normoxia, T1a was 1819±142ms, which was shortened to 1522±100ms during maximal hyperoxia, and the relationship between T1a and PETO2 was linear.
Hyperoxia gas mixture breathing, defined as fractional oxygen in inspired air (FiO2)>20.9%, is an isometabolic stimulus commonly used for calibrated fMRI studies1,2. Hyperoxia increases the oxygen carrying capacity of blood via oxygen dissolved in plasma. Oxygen itself is paramagnetic; therefore, the increased dissolved oxygen, which is proportional to FiO2, shortens the longitudinal relaxation time (T1) of blood3. Accurate knowledge of arterial blood T1 (T1a) is especially important for quantification of perfusion via arterial spin labeling (ASL)4.
Typically, in vivo quantification of T1a using traditional inversion recovery (IR) methods is not feasible due to transit of blood between the inversion pulse and image acquisition. Here, the problem of flow is overcome using an intermittent arterial occlusion protocol where blood flow is suspended in the femoral artery and vein during image acquisition, thereby allowing for quantification of T1a in vivo using standard methods.
Experiment: In this IRB approved study, data were acquired at 3T (Siemens) in ten subjects (30.5±3.8 years, 6 male). Figure 1 summarizes the experimental protocol. Subjects were supine with their right leg centered in an 8ch transmit-receive knee coil. A pneumatic tourniquet (Hokanson) was secured around the thigh, and pressure in the cuff was alternated between 215mmHg (inflated) and 0mmHg (deflated) during the image acquisition, yielding intermittent arterial occlusion. The image acquisition plane was prescribed distal to the cuff, perpendicular to the femoral artery to mitigate partial volume effects. For each level of hyperoxia, an IR-bSSFP sequence (written in SequenceTree5) was used for data collection, and pressure in the cuff was rapidly deflated and re-inflated during the 8.3 s recovery time between bSSFP acquisition and inversion.
Hyperoxia levels were: (1) normoxia (FiO2~21%, partial pressure of end tidal oxygen (PETO2)=113mmHg), (2) PETO2=200mmHg (FiO2~33%), (3) PETO2=300mmHg (FiO2~48%), (4) PETO2=350mmHg (FiO2~55%), and (5) FiO2=100% (PETO2~670mmHg) (Figure 2). Hyperoxic gas was delivered via a two-way non-rebreathing valve with input from the RespirAct Gas Control System (Thornhill Research) for graded hyperoxia, or 100L Douglas bag for 100% hyperoxia. Hematocrit was measured at the end of the experiment.
Sequence: IR-bSSFP sequence parameters include: FOV=160×160mm2, slice thickness=8mm, resolution=1×1mm2, bSSFP TR/TE=3.50/1.75ms, flip angle=60°, linear ramp catalyzation, bSSFP duration=360ms, inversion times (TI)=25, 50, 100, 250, 500, 750, 1000, 1500, 2000, 3000, 5000 ms, recovery time=8.3s, total scan time=109s. Immediately after the last TI, the cuff was deflated and inflated a final time, and phase contrast data were acquired to confirm flow suspension.
Analysis: Regions of interest (ROIs) in the femoral artery (and vein, if visible) were drawn on the IR-bSSFP images and a three-parameter fit6,7 was used to estimate T1 for each condition in each subject.
A previous pilot study investigated use of a continuous arterial occlusion, however we noticed that the artery became progressively smaller throughout the image series, likely due to reduced intra-arterial pressure distal to the cuff. Therefore, even though arterial saturation should remain constant in stagnant arterial blood (since oxygen extraction occurs in the capillary bed), we opted to use an intermittent arterial flow suspension protocol to maintain sufficient vessel size.
The hyperoxic T1a reported herein is in good agreement with previous studies that have estimated T1a using unconventional ASL-based methods (1500±40ms in rats8 and 1490±90ms in humans9 at 100% FiO2). There was no change in venous blood T1 during hyperoxia, as expected since plasma-dissolved oxygen is negligible in venous blood10. In this relatively small sample, a significant correlation was not observed between hematocrit and T1a, however, it is expected that with increased power, this known association would be observed4. The quantified normoxic T1a is in fair agreement with prior reports6,7.